Evaluation of shear bond strength of orthodontic molar tubes bonded using hydrophilic primers. An in-vitro study
Abstract
Statement of Problem: Orthodontic bonding is an essential step that impacts greatly the
success of the treatment. Attachment de-bonding during treatment is inconvenient and costly
to both the orthodontist and the patient. Moisture contamination is considered the most
common cause for bond failure especially in the posterior region. Objective: To evaluate and
compare the shear bond strength (SBS) of orthodontic molar tubes bonded using two
hydrophilic primers to dry and saliva-contaminated enamel surfaces and to assess the mode
of their bond failure. Design: In vitro comparative experimental study. Materials and
Methods: A total of 60 extracted human mandibular molars were randomly divided into
three major groups according to the primer used, each consisting of 20 molars: XT group acts
as a control and bonded with the conventional hydrophobic Transbond XT primer, OS group
bonded with the hydrophilic Ortho Solo primer, AP group bonded with the hydrophilic
Assure Plus all surface bonding resin. Each major group was further divided into two
subgroups, of 10 molars each, according to presence or absence of saliva. All the specimens
were thermocycled 500 cycles between 5°C and 55°C. Shear forces were applied to the
specimens with a universal testing machine at a crosshead speed of 1mm/min and SBS was
measured in megapascals. The mode of failure was determined using the adhesive remnant
index (ARI). Data were analyzed using two-way analysis of variance (ANOVA) followed by
univariate analysis and Bonferroni post hoc tests. The significance level was set at P ≤0.05.
Results: The three tested primers did not show a significant difference in the mean SBS in
dry conditions; the mean SBS of OS and AP primers were 15.60 ± 5.879 MPa and 12.51 ±
2.583 MPa respectively which were comparable to that of the hydrophobic XT primer (12.76
± 2.952 MPa). In saliva-contaminated conditions, the mean SBS values were 10.41 ± 4.457
MPa and 9.22 ± 3.422 MPa for OS and AP primers respectively which were significantly
higher than that of XT primer (4.82 ± 2.050 MPa). When comparing the mean SBS for each group according to the bonding condition, it was significantly higher in dry bonding
compared to saliva-contaminated bonding for the three primers. In dry field, most of the bond
failures of the three primers were adhesive (score 3); whereas in saliva-contaminated field,
most of the failures were cohesive (score 1). Conclusion: Bonding under dry conditions
yielded the highest SBS for the three primers. Saliva contamination significantly decreased
the bond strength of both hydrophilic primers compared with dry conditions; however, the
values were above the clinically acceptable limit. The hydrophilic primers tested in the
present study can be successfully used for bonding orthodontic molars tubes under dry and
saliva-contaminated enamel surface conditions.
Keywords: Shear bond strength, Molar tubes, Hydrophilic primers, Saliva contamination,
Thermocycling.
Student(s)
Rima Ibrahim Hadrous
Supervisor(s)
Prof. Essam Osman and Prof. Joseph Bou Serhal